Hydroxylamine → 5-Diethylphosphono-2-furaldehyde oxime
반응식
[CH2:1]([O:3][P:4]([C:9]1[O:13][C:12]([CH:14]=O)=[CH:11][CH:10]=1)([O:6][CH2:7][CH3:8])=[O:5])[CH3:2].[NH2:16][OH:17].C([O-])(=O)C.[Na+]>C(O)C>[CH2:1]([O:3][P:4]([C:9]1[O:13][C:12]([CH:14]=[N:16][OH:17])=[CH:11][CH:10]=1)([O:6][CH2:7][CH3:8])=[O:5])[CH3:2]참가 물질
5
실험 절차
A solution of 5-diethylphosphono-2-furaldehyde (1 mmole) in ethanol was treated with hydroxylamine (1.1 mmole) and sodium acetate (2.2 mmole) at 25° C. for 12 h. Extraction and chromatography gave 5-diethylphosphono-2-furaldehyde oxime.
후처리
- extractionExtraction and chromatography
출처 및 근거
- ORD 기록
- ord-5878d65bc0a0425083231294af4e990c
- 출처 데이터셋
- uspto-grants-2005_11
- 특허 번호
- US06965033B2
반응 노트
불러오는 중…