HCID 22280189, 화합물 → 2,5-Dimethyl-4-thiocyanato-phenol

반응식

COC1C(SC#N)=CC(C)=C(O)C=1.COC(=O)C[O:18][C:19]1[CH:24]=[C:23]([CH3:25])[C:22]([S:26][C:27]#[N:28])=[CH:21][C:20]=1[CH3:29]>>[CH3:29][C:20]1[CH:21]=[C:22]([S:26][C:27]#[N:28])[C:23]([CH3:25])=[CH:24][C:19]=1[OH:18]

참가 물질

반응물 2

HCID 22280189HCID 22280189, 화합물

HCID 85845775HCID 85845775, 화합물

생성물 1

HCID 222800452,5-Dimethyl-4-thiocyanato-phenol

실험 절차

The title compound was prepared in a manner analogous to compound 1B. 400 MHz 1H NMR (DMSO-d6) δ 10.0 (s, 1H), 7.35 (s, 1H), 6.73 (s, 1H), 2.3 (s, 3H), 2.04 (s, 3H); MS m/z 180 (m+1). Preparation of (2,5-Dimethyl-4-thiocyanato-phenoxy)-acetic acid methyl ester (Compound WWB)

출처 및 근거

ORD 기록: ord-25031e1a76204c62ade45b72b495a53f
출처 데이터셋: uspto-grants-2005_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06964983B2

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