Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Propan-2-yl 2,3,3,3-tetrafluoro-2-(heptafluoropropoxy)propanoate → (CF3)2Cfococf(CF3)ocf2CF2CF3
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Propan-2-yl 2,3,3,3-tetrafluoro-2-(heptafluoropropoxy)propanoate | HCID 10177266 | — |
| 반응물 | (CF3)2Chococf(CF3)ocf2CF2CF3 | HCID 10277469 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | (CF3)2Cfococf(CF3)ocf2CF2CF3 | HCID 131724614 | — |
반응 단계
Further, the same operation was repeated once. The total amount of benzene injected was 0.219 g, and the total amount of R-113 injected was 21 ml. Further, nitrogen was supplied for 1.5 hours. The product was quantified by 19F-NMR, whereby the yield of the above identified compound to (CH3)2CHOCOCF(CF3)OCF2CF2CF3, was 48.1%, and the yield of (CF3)2CHOCOCF(CF3)OCF2CF2CF3 to (CH3)2CHOCOCF(CF3)OCF2CF2CF3, was 19.1%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06969776B2 |
| 출처 데이터셋 | uspto-grants-2005_11 |
| ORD ID | ord-b79f83f57f5546bc90cfd9bd875c024e |
| 출처 메모 | uspto-grants-2005_11 |