Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylformamide → 4-Benzyloxy-2-(trifluoromethyl)benzaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylformamide | HCID 6228 | — |
| 반응물 | 4-(Benzyloxy)-1-bromo-2-(trifluoromethyl)benzene | HCID 22273864 | — |
| 반응물 | Butyllithium | HCID 178418339 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 4-Benzyloxy-2-(trifluoromethyl)benzaldehyde | HCID 22273885 | — |
반응 단계
In analogy to the procedure described in example 8 c], 1-bromo-2-trifluoromethyl-4-(phenylmethoxy)-benzene was treated with n-BuLi and N,N-dimethylformamide in dry tetrahydrofuran to yield 4-benzyloxy-2-trifluoromethyl-benzaldehyde as colorless liquid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06969725B2 |
| 출처 데이터셋 | uspto-grants-2005_11 |
| ORD ID | ord-bc3bf74a827e44eba5c73ae78aa96eb5 |
| 출처 메모 | uspto-grants-2005_11 |