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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1065047생성일: 2026년 10월 27일

p-nitrophenol sodium salt → 1-Methyl-4-[2-(4-nitrophenoxy)ethyl]benzene

https://huagongshe.com/reaction/1065047

반응식

참여 물질

역할이름HCID투입량
반응물p-nitrophenol sodium saltHCID 13214—
반응물4-Methylphenethyl bromideHCID 570680—
용매DimethylformamideHCID 6228—
생성물1-Methyl-4-[2-(4-nitrophenoxy)ethyl]benzeneHCID 514292673.8%

반응 단계

2-(4-Methylphenyl)ethyl bromide (X: X=Br) (10 g, 0.05 mole) and sodium 4-nitrophenolate (XI) (8.1 g, 0.05 mole) were added to dimethylformamide (60 ml), and the mixture was reacted at 90° C. for 5 hours. Thereafter, the reaction mixture was treated in the same manner as in Example 12 to obtain 9.5 g of 4-[2-(4-methylphenyl)ethoxy]-nitrobenzene (VI) as white crystals (yield, 73.9%).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04328166
출처 데이터셋uspto-grants-1982_05
ORD IDord-e62dd0aa8a7f41d4a22d917b5c66675c
출처 메모uspto-grants-1982_05