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llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
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Trimethyloxonium hexachlorantimonate → 2-Methyl-3,4,5-trichloroisothiazolium hexachloroantimonate

HRID 1065126
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HRID 1065126 반응식
[Cl:1][C:2]1[S:6][N:5]=[C:4]([Cl:7])[C:3]=1[Cl:8].[Cl:9][Sb-:10]([Cl:15])([Cl:14])([Cl:13])([Cl:12])[Cl:11].[CH3:16][O+](C)C>CCOCC>[Cl:9][Sb-:10]([Cl:15])([Cl:14])([Cl:13])([Cl:12])[Cl:11].[CH3:16][N+:5]1[S:6][C:2]([Cl:1])=[C:3]([Cl:8])[C:4]=1[Cl:7]
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참가 물질

4

반응물 2

HCID 150258Trimethyloxonium hexachlorantimonateHCID 12333154Trichloroisothiazole

생성물 1

HCID 166957382-Methyl-3,4,5-trichloroisothiazolium hexachloroantimonate수율 73%

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

Trichloroisothiazole (10 ml) and trimethyloxonium hexachloroantimonate (7.9 g, 0.02 mol) were heated at 90° for 30 min. After cooling ether (150 ml) was added and the solid collected to yield 7.8 g (73%) of product, mp >240. Spectral data (NMR and IR) were consistent with the assigned structure.

후처리

  1. additionwas added
  2. customthe solid collected

출처 및 근거

ORD 기록
ord-1eaf539dd5af4bf89324dab8922549b1
출처 데이터셋
uspto-grants-1982_05
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04328347

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