참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Lead monoxide | HCID 14827 | — |
| 반응물 | Ammonium Oleate | HCID 6435897 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | Lead stearate | HCID 61258 | — |
반응 단계
Separately, 3.5 l of warm water maintained at 70° C. was charged in a stainless steel beaker having a capacity of 10 l, and 419 g of stearic acid was added and dissolved under heating. Then, 24.0 cc of 7 N aqueous ammonia was dropped to the solution and the mixture was stirred and homogeneously emulsified to form an ammonia soap liquid. Separately, 725 cc of a lead monoxide slurry (PbO-DS) having a concentration of 680 g/l, 1 l of water and 14.2 cc of acetic acid having a concentration of 2.7 moles/liter were charged in a high-speed stirrer-equipped stainless steel vessel having a capacity of 10 l, and the mixture was maintained at 70° C. The above-mentioned ammonia soap liquid was added to this lead monoxide slurry and reaction was carried out under agitation to form a lead stearate slurry.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04329182 |
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| 출처 데이터셋 | uspto-grants-1982_05 |
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| ORD ID | ord-72d1730077364948b7eb6e358c9b16df |
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| 출처 메모 | uspto-grants-1982_05 |
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