Homophthalic acid → HCID 12593065, 화합물

HRID 1065493

반응식

HRID 1065493 반응식
[C:1]([CH2:4][C:5]1[CH:13]=[CH:12][CH:11]=[CH:10][C:6]=1[C:7]([OH:9])=O)(O)=O.[NH2:14][C:15]([CH3:19])([CH3:18])[CH2:16][SH:17].C([O-])(=O)C.[Na+]>ClC1C=CC=CC=1Cl>[CH3:18][C:15]1([CH3:19])[N:14]2[C:7](=[O:9])[C:6]3[CH:10]=[CH:11][CH:12]=[CH:13][C:5]=3[CH:4]=[C:1]2[S:17][CH2:16]1

참가 물질

5

반응물 3

HCID 66643Homophthalic acidHCID 517045Sodium AcetateHCID 5210402-Amino-2-methylpropane-1-thiol

생성물 1

HCID 12593065HCID 12593065, 화합물

시약·촉매·용매 1

HCID 72391,2-Dichlorobenzene용매

실험 절차

By following the same procedure as in Example 49 using a mixture of 240 mg. of 2-carboxymethylbenzoic acid, 300 mg. of 2-amino-2-methylpropanethiol, 164 mg. of sodium acetate, and 5 ml. of o-dichlorobenzene, 120 mg. of 3,3-dimethyl-5-oxo-2,3-dihydro-5H-thiazolo[3,2-b]isoquinoline was obtained.

후처리

  1. additiona mixture of 240 mg

출처 및 근거

ORD 기록
ord-93291bbc12484e1d887ab4d4321b7e72
출처 데이터셋
uspto-grants-1982_05
특허 번호
US04329455

연결된 노트

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