Butyl Isothiocyanate → HCID 178448907, 화합물

HRID 1066109

반응식

HRID 1066109 반응식
[NH2:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[S:9]([NH2:12])(=[O:11])=[O:10].[CH2:13]([N:17]=[C:18]=S)[CH2:14][CH2:15][CH3:16]>C(OCC)(=O)C>[Cl:8][C:6]1[CH:5]=[CH:4][C:3]2[S:9](=[O:11])(=[O:10])[N:12]=[C:18]([NH:17][CH2:13][CH2:14][CH2:15][CH3:16])[NH:1][C:2]=2[CH:7]=1

참가 물질

4

반응물 2

HCID 11613Butyl IsothiocyanateHCID 777902-Amino-4-chlorobenzenesulphonamide

생성물 1

HCID 178448907HCID 178448907, 화합물

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

실험 절차

The title compound was prepared from 2-amino-4-chlorobenzenesulfonamide and butyl isothiocyanate by a method analogous to the one described in Example 4; m.p. 267-269° C. (ethyl acetate); 1H-NMR (DMSO-d6): δ 0.90 (t, 3H, CH3), 1.24-1.60 (m, 4H, CH2CH2), 3.21 (q, 2H, NHCH2), 7.2-7.4 (m, 3H, ArH+NH), 7.68 (d, 1H, ArH), 10.55 (br.s, 1H, NH); MS: m/e 287-289 (M+); (C11H14N3Cl1O2S1) calc. C, 45.91; H, 4.91; N, 14.60; found C, 45.92; H, 5.12; N, 14.46.

출처 및 근거

ORD 기록
ord-bfeb011780f8430b9171d66eaafbfea3
출처 데이터셋
uspto-grants-2001_06
특허 번호
US06242443B1

연결된 노트

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