2-Amino-4-chlorobenzenesulphonamide → HCID 178444755, 화합물

HRID 1066110

반응식

HRID 1066110 반응식
[NH2:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[S:9]([NH2:12])(=[O:11])=[O:10].[CH2:13]([N:19]=[C:20]=S)[CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]>C(OCC)(=O)C>[Cl:8][C:6]1[CH:5]=[CH:4][C:3]2[S:9](=[O:11])(=[O:10])[N:12]=[C:20]([NH:19][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])[NH:1][C:2]=2[CH:7]=1

참가 물질

4

반응물 2

HCID 777902-Amino-4-chlorobenzenesulphonamideHCID 78120Hexyl isothiocyanate

생성물 1

HCID 178444755HCID 178444755, 화합물

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

실험 절차

The title compound was prepared from 2-amino-4-chlorobenzenesulfonamide and hexyl isothiocyanate by a method analogous to the one described in Example 4; m.p. 244-247° C. (ethyl acetate); 1H-NMR (DMSO-d6): δ 0.88 (distorted t, 3H, CH3), 1.31 (m, 6H, 3×CH2), 1.53 (m, 2H, CH2), 3.22 (q, 2H, NHCH2), 7.2-7.4 (m, 3H, ArH+NH), 7.68 (d, 1H, ArH), 10.55 (br.s, 1H, NH); MS: m/e 315/317 (M+); (C13H18N3Cl1O2S1) caic. C, 49.44; H, 5.74 N, 13.31; found C, 49.59; H, 6.01; N, 13.25.

출처 및 근거

ORD 기록
ord-3e61a1b5ef80410c878c9d5766671f88
출처 데이터셋
uspto-grants-2001_06
특허 번호
US06242443B1

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