참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | p-Toluenesulfonic acid | HCID 6101 | — |
| 반응물 | 16-Methylheptadecanoic Acid | HCID 21859 | — |
| 생성물 | Methyl 16-methylheptadecanoate | HCID 110444 | — |
반응 단계
About 780 grams of isostearic acid (acid number=194.4), 1 gram of p-toluenesulfonic acid were charged to a flask equipped with a heating mantle, stirrer, sub-surface inlet tube with a nitrogen purge and a condenser. The contents of the flask were heated under nitrogen flow to 117° C. About 400 grams of methanol were then added via the sub-surface inlet tube over 3.5 hours (acid number=9.6), 200 grams of additional methanol were added and the reaction continued for another 1.5 hours to obtain a final acid number of 0.6.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06242620B1 |
|---|
| 출처 데이터셋 | uspto-grants-2001_06 |
|---|
| ORD ID | ord-96c91d37ee5548f2ab674ac273685ede |
|---|
| 출처 메모 | uspto-grants-2001_06 |
|---|
