참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | Methyl 3-Hydroxy-2-methylene-3-phenylpropionate | HCID 9942369 | — |
| 생성물 | Methyl 2-[(acetyloxy)methyl]-3-phenylprop-2-enoate | HCID 53678280 | 100.8% |
반응 단계
Methyl 3-hydroxy-2-methylene-3-phenylpropionate (1.7836 g, 9.279 mmols) was dissolved in 1.75 ml (18.55 mmols) of acetic anhydride, and 0.03 ml of sulfuric acid were added thereto. The mixture was stirred at 100° C. for 4 hours. After the completion of the reaction, the reaction solution was concentrated under reduced pressure to obtain 2.1917 g of a crude product of the above title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06242635B1 |
|---|
| 출처 데이터셋 | uspto-grants-2001_06 |
|---|
| ORD ID | ord-bf7fac68b2be4e1680fe67d00927874a |
|---|
| 출처 메모 | uspto-grants-2001_06 |
|---|
