Butylimidazole → 1-Butyl-3-methylimidazolium tetrafluoroborate

HRID 1067042

반응식

HRID 1067042 반응식
[F:1][B-:2]([F:5])([F:4])[F:3].[CH3:6][O+](C)C.[CH2:10]([N:14]1[CH:18]=[CH:17][N:16]=[CH:15]1)[CH2:11][CH2:12][CH3:13]>ClCCCl>[F:1][B-:2]([F:5])([F:4])[F:3].[CH3:6][N+:16]1[CH:17]=[CH:18][N:14]([CH2:10][CH2:11][CH2:12][CH3:13])[CH:15]=1

참가 물질

4

반응물 2

HCID 61347ButylimidazoleHCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)

생성물 1

HCID 27341781-Butyl-3-methylimidazolium tetrafluoroborate

시약·촉매·용매 1

HCID 111,2-Dichloroethane용매2회

실험 절차

The procedure of Example 2 was followed. 3 g of trimethyloxonium tetrafluoroborate in suspension in 10 ml of 1,2-dichloroethane was added to 2.7 ml of N-butylimidazole in 10 ml of 1,2-dichloroethane. The mixture was stirred for 4 hours at room temperature. The remaining solvent was evaporated off under vacuum using a vane pump. A colorless liquid was obtained.

후처리

  1. customThe remaining solvent was evaporated off under vacuum
  2. customA colorless liquid was obtained

출처 및 근거

ORD 기록
ord-83f6c74419bd4ec6866c10e468d98ae4
출처 데이터셋
uspto-grants-2001_06
특허 번호
US06245918B1

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