HCID 178440796, 화합물 → HCID 178440797, 화합물

HRID 1067668노트

반응식

HRID 1067668 반응식
[NH:1]1[CH:5]=[C:4]([CH:6]([CH2:9][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[CH:7]=[CH2:8])[N:3]=[CH:2]1>CO.[Pd]>[NH:1]1[CH:5]=[C:4]([CH:6]([CH2:9][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[CH2:7][CH3:8])[N:3]=[CH:2]1

참가 물질

4

반응물 1

HCID 178440796HCID 178440796, 화합물

생성물 1

HCID 178440797HCID 178440797, 화합물

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 887Methanol용매

실험 절차

3 mmol of (1H-imidazol-4-yl)-4-phenyl-1-butene (Example 51) are dissolved in 50 ml of methanol. 70 mg Pd/C (10%) are added, and reduction is carried out for 12 hours at a pressure of 10 bar under hydrogen.

출처 및 근거

ORD 기록
ord-eb3637299df34c768630c543509539fd
출처 데이터셋
uspto-grants-2001_06
특허 번호
US06248765B1

반응 노트

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