Guanidine Hydrochloride → HCID 178502883, 화합물
반응식
CO[N:3]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[C:4]1[C:12]([O:14]C)=O.[ClH:16].[NH2:17][C:18]([NH2:20])=[NH:19].[CH3:21][O-:22].[Na+]>CO>[ClH:16].[CH3:21][O:22][NH:19][C:18]([NH2:20])=[N:17][C:12]([C:4]1[NH:3][C:11]2[C:6]([CH:5]=1)=[CH:7][CH:8]=[CH:9][CH:10]=2)=[O:14]참가 물질
5
실험 절차
The reaction was carried out in a manner similar to Example 1 except for using 0.46 g (2.24 mmol) of methyl 1-methoxy-2-indolecarboxylate, 2.14 g (22.4 mmol) of guanidine hydrochloride and 15 ml of a methanol solution of 1.21 g (22.4 mmol) of sodium methoxide. Thus 0.15 g (24.9%) of 1-methoxy-2-indoloylguanidine hydrochloride was obtained.
출처 및 근거
- ORD 기록
- ord-aa527bd871fb4916971764163de8a924
- 출처 데이터셋
- uspto-grants-2001_06
- 특허 번호
- US06248772B1
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