Isopropyl trifluoromethanesulfonate → HCID 54017818, 화합물

HRID 1067935노트

반응식

[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9](=[O:16])[CH2:10][N:11]1[CH:15]=[N:14][N:13]=[N:12]1.O([CH:25]([CH3:27])[CH3:26])S(C(F)(F)F)(=O)=O>>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9]([O:16][CH:25]([CH3:27])[CH3:26])=[CH:10][N:11]1[CH:15]=[N:14][N:13]=[N:12]1

참가 물질

반응물 2

HCID 10877967Isopropyl trifluoromethanesulfonate

HCID 21195251HCID 21195251, 화합물

생성물 1

HCID 54017818HCID 54017818, 화합물

실험 절차

Analogously to Example 7a,b, after reacting 1-(2,4-dichlorophenyl)-2-tetrazol-1-yl-ethanone with isopropyl triflate there was obtained 1-[2-(2,4-dichloro-phenyl)-2-isopropoxy-vinyl]-1H-tetrazole as a white powder with m.p. 82° C.

출처 및 근거

ORD 기록: ord-1272af68d41b40c391667c22762bb7dc
출처 데이터셋: uspto-grants-2001_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06248901B1

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