Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N,N,2-Trimethylaniline → p-Methoxybenzyltrichlorosilane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N,N,2-Trimethylaniline | HCID 11869 | — |
| 반응물 | Trichlorosilane | HCID 24811 | — |
| 반응물 | 4-Methyloxybenzyl chloride | HCID 69993 | — |
| 생성물 | p-Methoxybenzyltrichlorosilane | HCID 11482253 | 11.3% |
반응 단계
In the same apparatus and procedure as Example 1 above, 0.06 g (0.45 mmol) of N,N-dimethyltoluidine, 0.7 g (4.5 mmol) of 4-methoxybenzyl chloride, and 3.05 g (22.5 mmol) of trichlorosilane were reacted at 200+ C. for 15 hrs. The resulting mixture was distilled to give 0.13 g of (4-methoxybenzyl)trichlorosilane (yield; 11%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06251057B1 |
| 출처 데이터셋 | uspto-grants-2001_06 |
| ORD ID | ord-386dd98b71b5429bb4eb1c57d306cbbf |
| 출처 메모 | uspto-grants-2001_06 |