Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → 1,3-Bis(trichlorosilyl)propane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 1,3-Dichloropropane | HCID 8881 | — |
| 반응물 | Trichlorosilane | HCID 24811 | — |
| 생성물 | 1,3-Bis(trichlorosilyl)propane | HCID 11243856 | 9% |
반응 단계
In the same apparatus and procedure as Example 1 above, 0.048 g (0.47 mmol) of triethylamine, 0.6 g (4.7 mmol) of 1,3-dichloropropane, and 3.18 g (23.5 mmol) of trichlorosilane were reacted at 200° C. for 15 hrs. The resulting mixture was distilled to give 0.13 g of 1,3-bis(trichlorosilyl)propane (yield; 9%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06251057B1 |
| 출처 데이터셋 | uspto-grants-2001_06 |
| ORD ID | ord-557893ce53c2404b9451f329735f3300 |
| 출처 메모 | uspto-grants-2001_06 |