3-Nitrophenylboronic Acid → HCID 11529752, 화합물

HRID 1069072

반응식

HRID 1069072 반응식
Br[C:2]1[CH:11]=[CH:10][C:5]([C:6]([O:8][CH3:9])=[O:7])=[CH:4][C:3]=1[C:12]([O:14][CH3:15])=[O:13].[N+:16]([C:19]1[CH:20]=[C:21](B(O)O)[CH:22]=[CH:23][CH:24]=1)([O-:18])=[O:17]>C1C=CC([P]([Pd]([P](C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)([P](C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)[P](C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)=CC=1>[CH3:15][O:14][C:12]([C:3]1[C:2]([C:23]2[CH:22]=[CH:21][CH:20]=[C:19]([N+:16]([O-:18])=[O:17])[CH:24]=2)=[CH:11][CH:10]=[C:5]([C:6]([O:8][CH3:9])=[O:7])[CH:4]=1)=[O:13]

참가 물질

4

반응물 2

HCID 16773-Nitrophenylboronic AcidHCID 2824912Dimethyl 4-bromoisophthalate

생성물 1

HCID 11529752HCID 11529752, 화합물

시약·촉매·용매 1

HCID 178418397HCID 178418397, 화합물촉매

실험 절차

Electrospray MS (positive ion): (M+Na) 338; from dimethyl 4-bromoisophthalate (1.26 g), 3-nitrophenylboronic acid (795 mg) and tetrakis(triphenylphosphine)palladium(0) (167 mg).

출처 및 근거

ORD 기록
ord-7ef1446249904566a6f2f067940b98f0
출처 데이터셋
uspto-grants-2001_06
특허 번호
US06251925B1

연결된 노트

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