3-Nitrophenylboronic Acid → HCID 16125934, 화합물

HRID 1069075

반응식

HRID 1069075 반응식
[CH2:1]([O:3][C:4]([C:6]1[CH:11]=[CH:10][N:9]=[C:8](Br)[CH:7]=1)=[O:5])[CH3:2].[N+:13]([C:16]1[CH:17]=[C:18](B(O)O)[CH:19]=[CH:20][CH:21]=1)([O-:15])=[O:14]>>[CH2:1]([O:3][C:4]([C:6]1[CH:11]=[CH:10][N:9]=[C:8]([C:20]2[CH:19]=[CH:18][CH:17]=[C:16]([N+:13]([O-:15])=[O:14])[CH:21]=2)[CH:7]=1)=[O:5])[CH3:2]

참가 물질

3

반응물 2

HCID 16773-Nitrophenylboronic AcidHCID 3847769Ethyl 2-bromoisonicotinate

생성물 1

HCID 16125934HCID 16125934, 화합물

실험 절차

Electrospray MS (positive ion): (M+H) 272.8; from 2-bromo4-pyridinecarboxylic acid ethyl ester (900 mg), tetrakis(triphenylphosphine)paliadium (136 mg), and 3-nitrophenylboronic acid (783 mg).

출처 및 근거

ORD 기록
ord-27722b9457f94597a2204c9f2a93a4fc
출처 데이터셋
uspto-grants-2001_06
특허 번호
US06251925B1

연결된 노트

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