Phenyl isocyanate → HCID 22390756, 화합물

HRID 1070737노트

반응식

HRID 1070737 반응식
[NH:1]([CH2:5][CH2:6][OH:7])[CH2:2][CH2:3][OH:4].[C:8]1([N:14]=[C:15]=[O:16])[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1>ClCCl>[OH:4][CH2:3][CH2:2][N:1]([CH2:5][CH2:6][OH:7])[C:15]([NH:14][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)=[O:16]

참가 물질

4

반응물 2

HCID 7672Phenyl isocyanateHCID 8113Diethanolamine

생성물 1

HCID 22390756HCID 22390756, 화합물

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

0.163 mol of diethanolamine dissolved in 160 ml of dichloromethane is added, at 10° C., to a solution of 0.168 mol of phenyl isocyanate. After reacting for 1 hour at 10° C. and then for 12 hours at ambient temperature, the reaction mixture is concentrated under reduced pressure.

후처리

  1. waitfor 12 hours at ambient temperature
  2. concentrationthe reaction mixture is concentrated under reduced pressure

출처 및 근거

ORD 기록
ord-2a9ac55dc25248ac9c46afd98402df71
출처 데이터셋
uspto-grants-2005_06
특허 번호
US06903103B2

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