참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | 1,3-Dioxane | HCID 10450 | — |
| 반응물 | Sodium Acetate | HCID 517045 | — |
| 생성물 | 1-Acetoxy-3-acetoxymethoxypropane | HCID 12480848 | 50,174.398% |
반응 단계
To a mixture of 1,3-dioxan (3 ml, 0.035 mmol) and acetic anhydride (3.3 ml, 0.035 mmol) at 0° C., was added a drop of concentrated sulphuric acid. The mixture was then stirred for 14 h at 20° C., added with sodium acetate (2 g) and filtrated. The residue, distilled in vacuo (120° C., 16 mmHg), gave 1-acetoxy-3-acetoxymethoxypropane (3.34 g, 50%) as a colorless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06911450B1 |
|---|
| 출처 데이터셋 | uspto-grants-2005_06 |
|---|
| ORD ID | ord-a3b64d75c18e47ab9ee7d9cf59ae7f5b |
|---|
| 출처 메모 | uspto-grants-2005_06 |
|---|
