참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sulfuryl chloride | HCID 24648 | — |
| 반응물 | Benzyl Phenyl Ether | HCID 70352 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 4-(Benzyloxy)benzene-1-sulfonyl chloride | HCID 4738385 | — |
반응 단계
A 1.12 portion of anhydrous DMF is cooled to 0° C. and treated dropwise with 2.06 g of sulfuryl chloride. The resulting suspension is stirred for 30 min., then treated with 1.50 g of benzyl phenyl ether. The mixture is heated at 90° C. for 3 h, then cooled, extracted with brine and methylene chloride, and dried over MgSO4. Chormotography on silica gel (i-PrOH/hexanes) yields 4-benzyloxybenzenesulfonyl chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05723490 |
|---|
| 출처 데이터셋 | uspto-grants-1998_03 |
|---|
| ORD ID | ord-7b357d5bf4334f0fb405475a558ece52 |
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| 출처 메모 | uspto-grants-1998_03 |
|---|
