Triethylamine → HCID 14853717, 화합물
반응식
[NH2:1][C:2]1[C:3]([NH:8][CH:9]([CH3:11])[CH3:10])=[N:4][CH:5]=[CH:6][CH:7]=1.C(N(CC)CC)C.[C:19](Cl)([C:21](OCC)=[O:22])=[O:20]>O1CCCC1>[CH:9]([N:8]1[C:19](=[O:20])[C:21](=[O:22])[NH:1][C:2]2[CH:7]=[CH:6][CH:5]=[N:4][C:3]1=2)([CH3:11])[CH3:10]참가 물질
5
실험 절차
To a stirred solution of 3-amino-2-isopropylamino-pyridine (2.0 g, 10.6 mmole) and triethylamine (4.8 ml, 34.6 mmole) in tetrahydrofuran (30 ml) was dropwise added ethoxalyl chloride (2.68 ml, 24 mmole). Stirring was continued for two hours after the addition. The mixture was filtered through a glass filter funnel and the filtrate was evaporated to give the title compound as white crystals. M.p. 246°-247° C.
후처리
- additionafter the addition
- filtrationThe mixture was filtered through a glass
- filtrationfilter funnel
- customthe filtrate was evaporated
출처 및 근거
- ORD 기록
- ord-c3efe739163c4d1384777b2d237f57ca
- 출처 데이터셋
- uspto-grants-1990_11
- 특허 번호
- US04968682
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