2,6-Naphthalenedicarbonyl dichloride → 2-Naphthoyl chloride

HRID 1074303

반응식

HRID 1074303 반응식
FC(F)(F)CCCCCCC1(C2C=CC(O)=CC=2)C=CC(C([O-])=O)=CC1.[CH:27]1[C:36]2[C:31](=[CH:32][C:33]([C:37]([Cl:39])=[O:38])=[CH:34][CH:35]=2)[CH:30]=[CH:29][C:28]=1C(Cl)=O>C(N(CC)CC)C>[CH:32]1[C:31]2[C:36](=[CH:27][CH:28]=[CH:29][CH:30]=2)[CH:35]=[CH:34][C:33]=1[C:37]([Cl:39])=[O:38]

참가 물질

4

반응물 2

HCID 34855962,6-Naphthalenedicarbonyl dichlorideHCID 867443591-Trifluoroheptyl-4'-hydroxybiphenyl-4-carboxylate

생성물 1

HCID 752462-Naphthoyl chloride

시약·촉매·용매 1

HCID 8471Triethylamine용매

실험 절차

The compound (III) is reacted with 2,6-naphthalene-dicarboxylic acid dichloride in the presence of triethyl amine to obtain 6-[3-trifluoromethylheptyloxycarbonyl)-biphenyl-4-oxycarbonyl]-naphthalene-2-carboxylic acid chloride (IV).

출처 및 근거

ORD 기록
ord-f65d1ac51a354ca2a96438f6958d1f65
출처 데이터셋
uspto-grants-1990_11
특허 번호
US04973738

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