HCID 20496709, 화합물 → HCID 20496693, 화합물
반응식
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][OH:16])=[CH:6][CH:5]=1)([O-])=O>[Pd].C(O)C>[NH2:1][C:4]1[CH:5]=[CH:6][C:7]([CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][OH:16])=[CH:8][CH:9]=1참가 물질
4
실험 절차
A solution was prepared from 8.5 g of 6-(4-nitrophenyl)hexanol and 150 ml of ethanol and 0.42 g of 10% Pd/C catalyst was added. The resulting mixture was shaken under hydrogen (2.7-3.3 atmospheres) at room temperature for 2 hours. The catalyst was then removed by filtration and the solvent was evaporated from the filtrate to leave a crude tan solid. The solid was recrystallized from ethyl acetate/hexane to give 6-(4-aminophenyl)hexanol.
후처리
- additionwas added
- customThe catalyst was then removed by filtration
- customthe solvent was evaporated from the filtrate
- customto leave a crude tan solid
- customThe solid was recrystallized from ethyl acetate/hexane
출처 및 근거
- ORD 기록
- ord-d313ee34a0984847b93b397f148dec61
- 출처 데이터셋
- uspto-grants-1983_07
- 특허 번호
- US04391818
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