1,1-Dimethoxyethyl(dimethyl)amine → HCID 70534846, 화합물

반응식

[C:1]([CH2:3][C:4]([NH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[CH2:13][CH3:14])=[O:5])#[N:2].CO[C:17](OC)([N:19]([CH3:21])[CH3:20])[CH3:18]>>[C:1](/[C:3](=[C:17](/[N:19]([CH3:21])[CH3:20])\[CH3:18])/[C:4]([NH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[CH2:13][CH3:14])=[O:5])#[N:2]

참가 물질

반응물 2

HCID 878351,1-Dimethoxyethyl(dimethyl)amine

HCID 7318832-cyano-N-(2-ethylphenyl)acetamide

생성물 1

HCID 70534846HCID 70534846, 화합물

실험 절차

As for Example 1, 2-cyano-2'-ethylacetanilide is heated with N,N-dimethylacetamide dimethylacetal to give 2-cyano-3-dimethylamino-2'-ethylcrotonanilide as colorless prisms, m.p. 79°-81.5° C.

출처 및 근거

ORD 기록: ord-426a7bef687844508f5f155957ada7fb
출처 데이터셋: uspto-grants-1983_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04393217

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