2-Mercaptobenzoic Acid → HCID 12763557, 화합물

HRID 1075181노트

반응식

HRID 1075181 반응식
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10]Cl)=[C:6]([C:12]([Cl:15])([Cl:14])[Cl:13])[CH:5]=1)([O-:3])=[O:2].[SH:16][C:17]1[CH:25]=[CH:24][CH:23]=[CH:22][C:18]=1[C:19]([OH:21])=[O:20]>>[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10][S:16][C:17]2[CH:25]=[CH:24][CH:23]=[CH:22][C:18]=2[C:19]([OH:21])=[O:20])=[C:6]([C:12]([Cl:15])([Cl:14])[Cl:13])[CH:5]=1)([O-:3])=[O:2]

참가 물질

3

반응물 2

HCID 54432-Mercaptobenzoic AcidHCID 127635554-Nitro-2-trichloromethylbenzenesulfenyl chloride

생성물 1

HCID 12763557HCID 12763557, 화합물수율 87.1%

실험 절차

61.4 g of 4-nitro-2-trichloromethylbenzenesulfenyl chloride are reacted with 32 g of 2-mercaptobenzoic acid by a method similar to that of Example 1. 74 g (87% of theory) of o-(4-nitro-2-trichloromethylphenyldithio)-benzoic acid of melting point 224° C., are obtained.

출처 및 근거

ORD 기록
ord-697aa4b81ce14a2d9e4e4381a134cc21
출처 데이터셋
uspto-grants-1983_07
특허 번호
US04395415

반응 노트

불러오는 중…