참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1-Bromo-3-chloropropane | HCID 8006 | — |
| 반응물 | N,N-Dimethylhexylamine | HCID 78090 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | HCID 85711135 | HCID 85711135 | — |
반응 단계
A 500 mL, 3-necked, round-bottomed flask equipped with air condensers and a magnetic stirring plate was charged with N,N-dimethylhexylamine (199.46 grams, 1.54 moles), 1-bromo-3-chloropropane (243.00 grams, 1.54 moles) and 250 mL of methanol The reaction was maintained at 65° C. for 24 hours. Solvent was removed by rotary evaporation under reduced pressure to yield a brown, viscous oil. Yield 445.8 grams (1.55 moles, 100%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05900475 |
|---|
| 출처 데이터셋 | uspto-grants-1999_05 |
|---|
| ORD ID | ord-baddc76a16574c178672bdf5acd2d27b |
|---|
| 출처 메모 | uspto-grants-1999_05 |
|---|
