Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → N-methyl-2H-3-isoquinolone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Sodium Bicarbonate | HCID 516892 | — |
| 반응물 | N-methyl-2H-3-isoquinolone sulfate | HCID 21541268 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | N-methyl-2H-3-isoquinolone | HCID 12435498 | — |
반응 단계
70 g. N-methyl-2H-3-isoquinolone sulfate are dissolved, under an atmosphere of nitrogen, in 900 ml. water. 75 g. sodium bicarbonate are added and the mixture is stirred with 500 ml. chloroform. By decantation, there is obtained a chloroform solution of N-methyl-2H-3-isoquinolone, which can be dried over anhydrous sodium sulfate and employed as such or concentrated for a further reaction.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03954771 |
| 출처 데이터셋 | uspto-grants-1976_05 |
| ORD ID | ord-c078a18486cf4a12876c27b719da7b99 |
| 출처 메모 | uspto-grants-1976_05 |