Acetone → HCID 12582637, 화합물

반응식

[CH2:1]([O:4][C:5]([N:7]1[CH2:18][CH2:17][C:10]2[N:11]=[N:12][C:13]([NH:15][NH2:16])=[CH:14][C:9]=2[CH2:8]1)=[O:6])[CH:2]=[CH2:3].[CH3:19][C:20]([CH3:22])=O>>[CH2:1]([O:4][C:5]([N:7]1[CH2:18][CH2:17][C:10]2[N:11]=[N:12][C:13]([NH:15][N:16]=[C:20]([CH3:22])[CH3:19])=[CH:14][C:9]=2[CH2:8]1)=[O:6])[CH:2]=[CH2:3]

참가 물질

반응물 2

HCID 180Acetone

HCID 12582636HCID 12582636, 화합물

생성물 1

HCID 12582637HCID 12582637, 화합물

실험 절차

A solution of 4 g of 3-hydrazino-5,6,7,8-tetrahydro-6-pyrido[4,3-c]pyridazinecarboxylic acid allyl ester in 40 cc of acetone is heated at reflux on a water bath for 30 minutes. The title compound has a M.P. 134°-136° (decomp.).

후처리

temperatureat reflux on a water bath for 30 minutes

출처 및 근거

ORD 기록: ord-454f39e9170b48c18489218914fb4e33
출처 데이터셋: uspto-grants-1976_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US03954754

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