Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrogen Sulfide → Bis dodecyl phenol sulphide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrogen Sulfide | HCID 402 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 2-Dodecylphenol | HCID 171144 | — |
| 반응물 | Sulfur | HCID 5362487 | — |
| 생성물 | Bis dodecyl phenol sulphide | HCID 86733380 | — |
반응 단계
A mixture of dodecyl phenol (1.0m., 262g.), sulphur (1.0m., 32g.) and caustic soda (8g.) was heated, with stirring, under nitrogen, at 160° C until the evolution of hydrogen sulphide ceased (42 hrs.). The caustic soda was neutralized with 10 ml. of phosphoric acid (SG = 1.75) and the mixture was then filtered. %S of Product = 5.85 (calc. = 5.8).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03954808 |
| 출처 데이터셋 | uspto-grants-1976_05 |
| ORD ID | ord-cab618fac034433f919109032ac0567e |
| 출처 메모 | uspto-grants-1976_05 |