Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-Methylanthranilic acid → 9-Methyl-5,6,7,8-tetrahydrocarbazole-1-carboxylic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-Methylanthranilic acid | HCID 67069 | — |
| 반응물 | 2-Bromocyclohexanone | HCID 11789758 | — |
| 생성물 | 9-Methyl-5,6,7,8-tetrahydrocarbazole-1-carboxylic acid | HCID 21399959 | 15% |
반응 단계
Under the conditions of Example 59, 2-bromocyclohexanone is reacted with the methyl ester of N-methylanthranilic acid. After recrystallization from methanol, the methyl ester of 9-methyl-5,6,7,8-tetrahydrocarbazole-1-carboxylic acid is obtained in a 15% yield, m.p. 56° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03956295 |
| 출처 데이터셋 | uspto-grants-1976_05 |
| ORD ID | ord-91a61c60fe79499f817ca274f3c7a212 |
| 출처 메모 | uspto-grants-1976_05 |