Dimethylamine → HCID 21486904, 화합물
반응식
[CH3:1][O:2][CH:3]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][N:9]=1)[C:4](OC)=[O:5].[CH3:14][NH:15][CH3:16]>C(O)C>[CH3:1][O:2][CH:3]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][N:9]=1)[C:4]([N:15]([CH3:16])[CH3:14])=[O:5]참가 물질
4
실험 절차
A mixture of 18.1 g. of methyl 2-methoxy-2-(2-pyridyl)acetate and 10 g. of dimethylamine in ethanol is stirred at room temperature for 26 hours. The mixture is concentrated, dissolved in chloroform and extracted with brine. The organic phase is dried over magnesium sulfate and filtered and the solvent is removed under reduced pressure to give 2-methoxy-N,N-dimethyl-2-(2-pyridyl)acetamide.
후처리
- additionA mixture of 18.1 g
- concentrationThe mixture is concentrated
- dissolutiondissolved in chloroform
- extractionextracted with brine
- dry with materialThe organic phase is dried over magnesium sulfate
- filtrationfiltered
- customthe solvent is removed under reduced pressure
출처 및 근거
- ORD 기록
- ord-41df02ac05e54de2b054dd8c3f855d99
- 출처 데이터셋
- uspto-grants-1976_05
- 특허 번호
- US03956494
반응 노트
불러오는 중…