Formaldehyde → HCID 21537633, 화합물

HRID 1076527

반응식

HRID 1076527 반응식
[C:1]([NH:4][CH2:5][C:6]([OH:8])=[O:7])(=[O:3])[NH2:2].[CH2:9]=O.[NH:11]1[CH2:16][CH2:15][O:14][CH2:13][CH2:12]1>>[O:14]1[CH2:15][CH2:16][N:11]([CH2:9][NH:2][C:1]([NH:4][CH2:5][C:6]([OH:8])=[O:7])=[O:3])[CH2:12][CH2:13]1

참가 물질

4

반응물 3

HCID 712FormaldehydeHCID 8083MorpholineHCID 10020Hydantoic acid

생성물 1

HCID 21537633HCID 21537633, 화합물

실험 절차

1 mol of N-carbamyl glycine and 1 mol of formol are mixed while stirring. This mixture is cooled with ice-bath and 1 mol of morpholine is added slowly while keeping the temperature at about 15°C during 30 feet and at about 50°C during the same time. After cooling the resulting mixture is evaporated until dry. The residue is a white colored paste. The yield of the reaction is 98 %.

후처리

  1. temperatureThis mixture is cooled with ice-bath
  2. customat about 15°C
  3. customat about 50°C
  4. temperatureAfter cooling the resulting mixture
  5. customis evaporated
  6. customuntil dry

출처 및 근거

ORD 기록
ord-a75a564e4b0c4094b9d9dd22f0e9e613
출처 데이터셋
uspto-grants-1976_05
특허 번호
US03957774

연결된 노트

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