Formaldehyde → HCID 86733424, 화합물

HRID 1076528

반응식

HRID 1076528 반응식
C[NH:2][C:3]([N:5]([CH2:9]CC)[CH2:6][CH2:7][CH3:8])=[O:4].C=O.[NH:14]1[CH2:19][CH2:18][O:17][CH2:16][CH2:15]1>>[O:17]1[CH2:18][CH2:19][N:14]([CH2:9][N:5]([CH2:6][CH2:7][CH3:8])[C:3]([NH2:2])=[O:4])[CH2:15][CH2:16]1.[CH3:9][N:5]([CH2:6][CH2:7][CH3:8])[C:3]([NH2:2])=[O:4]

참가 물질

4

반응물 3

HCID 712FormaldehydeHCID 8083MorpholineHCID 215877Urea, 1,1-dipropyl-3-methyl-2회

생성물 1

HCID 86733424HCID 86733424, 화합물

실험 절차

1 mol of N-methyl dipropylurea and 1 mol of formol in aqueous 30% solution are mixed. To this solution 1 mol of morpholine is slowly added while cooling. The stirring is maintained one hour after the end of the N-methyl dipropylurea addition. After evaporation to dryness a crystalline product is obtained which melts at 110°C. The yield of the reaction is 98%.

후처리

  1. temperaturewhile cooling
  2. temperatureThe stirring is maintained one hour
  3. customAfter evaporation to dryness a crystalline product
  4. customis obtained which melts at 110°C

출처 및 근거

ORD 기록
ord-6cd7fcff60ed43e0b748a5001dd441f9
출처 데이터셋
uspto-grants-1976_05
특허 번호
US03957774

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