Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Acid → Acetoacetic Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Acid | HCID 176 | — |
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | (+)-Limonene | HCID 440917 | — |
| 생성물 | Acetoacetic Acid | HCID 96 | — |
| 생성물 | (+)-Limonene | HCID 440917 | — |
반응 단계
This patent discloses a process in which the 1,2 epoxide of limonene is refluxed with acetic acid and acetic anhydride to yield the 1,2 diacetate of limonene and the excess of these esterification reagents is removed. The diester product of pyrolysed by heating at atmospheric pressure at an elevated temperature. The carvyl acetate is obtained by fractional distillation of the resulting mixture.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03957856 |
| 출처 데이터셋 | uspto-grants-1976_05 |
| ORD ID | ord-4f678fd0b26f419a9e8c06c81a8a3a47 |
| 출처 메모 | uspto-grants-1976_05 |