Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Trichloroethylene → 2-METHYL-4,5,alpha,beta-TETRACHLOROSTYRENE
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Trichloroethylene | HCID 6575 | — |
| 반응물 | Benzene, 1,2-dichloro-4-methyl- | HCID 7256 | — |
| 반응물 | Aluminum(III) Chloride | HCID 6451240 | — |
| 생성물 | 2-METHYL-4,5,alpha,beta-TETRACHLOROSTYRENE | HCID 54418847 | — |
반응 단계
A mixture containing 131.5 g (1.0 mole), of trichloroethylene, 80.5 (0.5 mole) of 3,4-dichlorotoluene and 5 g. of aluminum chloride was stirred and heated at reflux for 2 hours. The reaction mixture was then washed with concentrated HCl, then with water until neutral, dried and distilled. 42.7 grams of product was collected, having a boiling point of 97°-102°C at 0.5 mm Hg pressure.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03957891 |
| 출처 데이터셋 | uspto-grants-1976_05 |
| ORD ID | ord-d4be8981b50d4d08a51b74a624717a0e |
| 출처 메모 | uspto-grants-1976_05 |