Oxalyl chloride → HCID 18999946, 화합물

HRID 1077054노트

반응식

HRID 1077054 반응식
[CH3:1][CH:2]([CH3:10])[CH2:3][CH2:4][C:5](=[O:9])[C:6](O)=[O:7].C(Cl)(=O)C([Cl:14])=O>>[CH3:1][CH:2]([CH3:10])[CH2:3][CH2:4][C:5](=[O:9])[C:6]([Cl:14])=[O:7]

참가 물질

3

반응물 2

HCID 65578Oxalyl chlorideHCID 1293965126395-06-2

생성물 1

HCID 18999946HCID 18999946, 화합물

실험 절차

reacting 5-methyl-2-oxohexanoic acid with at least a 10% excess of the stoichiometric amount of oxalyl chloride under anhydrous conditions at a temperature of 25° to 60° C. for from 40 to 60 hours to form 5-methyl-2-oxohexanoyl chloride;

후처리

  1. customat a temperature of 25° to 60° C.
  2. customfor from 40 to 60 hours

출처 및 근거

ORD 기록
ord-a6d18e3e0db94cb7a5a78c642e8e8b44
출처 데이터셋
uspto-grants-1976_05
특허 번호
US03959312

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