참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Oxalic Acid | HCID 971 | — |
| 반응물 | HCID 178419084 | HCID 178419084 | — |
| 촉매 | Niobium potassium oxide | HCID 160967 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 178526029 | HCID 178526029 | — |
반응 단계
Granulated alumina (8 - 16 mesh) is heated at 1300°C. for 4 hours. Potassium niobate (4K2O.3Nb2O5.16H2O) and vanadium pentoxide are suspended in 5 parts of water, heated to 80°C., and oxalic acid is added slowly to obtain a blue-colored vanadium oxalate solution. Sodium carbonate is added and the alumina is also placed in the solution. The mixture is dried over a water bath with agitation. While air is pumped in, it is indurated in a furnace at 400°C. for 16 hours to obtain the catalyst ready for use after cooling.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US03959336 |
|---|
| 출처 데이터셋 | uspto-grants-1976_05 |
|---|
| ORD ID | ord-a044738a2e224cfe80529a948e354241 |
|---|
| 출처 메모 | uspto-grants-1976_05 |
|---|
