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Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) → HCID 21993376, 화합물

HRID 1077408
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HRID 1077408 반응식
[F:1][B-:2]([F:5])([F:4])[F:3].[CH3:6][O+](C)C.[CH3:10][C:11]1[CH:16]=[C:15]([CH3:17])[N:14]=[C:13]([CH:18]=[CH2:19])[CH:12]=1>C(Cl)Cl>[F:1][B-:2]([F:5])([F:4])[F:3].[CH3:6][N+:14]1[C:15]([CH3:17])=[CH:16][C:11]([CH3:10])=[CH:12][C:13]=1[CH:18]=[CH2:19]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 2735153Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1)HCID 112288262-ethenyl-4,6-dimethyl-pyridine

생성물 1

HCID 21993376HCID 21993376, 화합물

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

Trimethyloxonium tetrafluoroborate (0.50 g; 3.76×10-3 mol) is added in one portion to a solution of 4,6-dimethyl-2-vinylpyridine (0.61 g; 4.13×10-3 mol) in 4.0 ml of methylene chloride under an inert atmosphere. The suspension is left to react for 2 h at 25° C. The suspension is filtered and the product is dried under vacuum. Yield=0.162 g (18%), white crystals.

후처리

  1. waitThe suspension is left
  2. customto react for 2 h at 25° C
  3. filtrationThe suspension is filtered
  4. customthe product is dried under vacuum

출처 및 근거

ORD 기록
ord-704950196d9549a6bb4494ebabfcb54d
출처 데이터셋
uspto-grants-1996_08
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US05543298

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