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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1077482생성일: 2026년 10월 24일

5,6-Diamino-1,3-diethyluracil → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(2,3-dimethyl-4-methoxy)phenyl)ethenyl)-, (E)-

https://huagongshe.com/ko/reaction/1077482

반응식

참여 물질

역할이름HCID투입량
반응물5,6-Diamino-1,3-diethyluracilHCID 4572133—
반응물4-Methoxy-2,3-dimethylcinnamic acidHCID 53401770—
생성물1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(2,3-dimethyl-4-methoxy)phenyl)ethenyl)-, (E)-HCID 644885717.2%

반응 단계

Substantially the same procedure as in Reference Example 70 was repeated using 2.5 g (12.6 mmol) of 5,6-diamino-1,3-diethyluracil and 2.9 g (13.9 mmol) of 4-methoxy-2,3-dimethylcinnamic acid. Then, the resultant crude crystals were recrystallized from ethanol/water to give 0.80 g (yield 17%) of Compound 81 as white crystals.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05543415
출처 데이터셋uspto-grants-1996_08
ORD IDord-36fd0cfe10ae46e195ee26c7beed3208
출처 메모uspto-grants-1996_08