Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5,6-Diamino-1,3-dimethyluracil → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-dimethyl-8-(2-(2,5-dimethyl-4-methoxyphenyl)ethenyl)-, (E)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5,6-Diamino-1,3-dimethyluracil | HCID 79501 | — |
| 반응물 | 4-Methoxy-2,5-dimethylcinnamic acid | HCID 5199898 | — |
| 생성물 | 1H-Purine-2,6-dione, 3,7-dihydro-1,3-dimethyl-8-(2-(2,5-dimethyl-4-methoxyphenyl)ethenyl)-, (E)- | HCID 6448977 | 20% |
반응 단계
Substantially the same procedure as in Reference Example 70 was repeated using 1.0 g (5.88 mmol) of 5,6-diamino-1,3-dimethyluracil and 1.33 g (6.45 mmol) of 4-methoxy-2,5-dimethylcinnamic acid. Then, the resultant crude crystals were recrystallized from dimethylformamide to give 393 mg (yield 20%) of Compound 101 as pale yellow grains.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05543415 |
| 출처 데이터셋 | uspto-grants-1996_08 |
| ORD ID | ord-c63a778b940443f6b736e9107aca4b8c |
| 출처 메모 | uspto-grants-1996_08 |