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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1077526생성일: 2026년 10월 26일

3-(4-Phenylphenyl)prop-2-enoic acid → 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(1,1'-biphenyl)-4-ylethenyl)-1,3-diethyl-, (E)-

https://huagongshe.com/reaction/1077526

반응식

참여 물질

역할이름HCID투입량
반응물3-(4-Phenylphenyl)prop-2-enoic acidHCID 25492—
반응물5,6-Diamino-1,3-diethyluracilHCID 4572133—
생성물1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(1,1'-biphenyl)-4-ylethenyl)-1,3-diethyl-, (E)-HCID 6448939—

반응 단계

Substantially the same procedure as in Reference Example 70 was repeated using 2.50 g (12.6 mmol) of 5,6-diamino-1,3-diethyluracil and 3.12 g (13.9 mmol) of 4-phenylcinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane/water to give 1.90 g (yield of Compound 170 as yellow flocculent precipitates.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05543415
출처 데이터셋uspto-grants-1996_08
ORD IDord-a569332d5fb64b4696d400fba9a449a5
출처 메모uspto-grants-1996_08