Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenyltrichlorosilane → Dichlorodiphenylsilane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenyltrichlorosilane | HCID 7372 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 촉매 | Dichloro(phenyl)silane | HCID 74207 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | Dichlorodiphenylsilane | HCID 6627 | 253.1% |
반응 단계
Triethylamine (3.9 g) was added to a flask containing 83.3 g of the crude product mixture described in Example 1. This mixture was stripped by the process described in Example 1. The volatiles were condensed and analyzed by GC-TCD. About 77.4 g of a liquid was recovered comprising 24.7 g of diphenyldichlorosilane (yield of 77 percent), 1.4 g of phenyldichlorosilane, 24.5 g of phenyltrichlorosilane, and 10.1 g of benzene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05545743 |
| 출처 데이터셋 | uspto-grants-1996_08 |
| ORD ID | ord-7290619a4c9d4a31a80dd0728247d398 |
| 출처 메모 | uspto-grants-1996_08 |