Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,4-Dimethylbenzoic acid → 3,4-Dimethylbenzoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,4-Dimethylbenzoic acid | HCID 12073 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 생성물 | 3,4-Dimethylbenzoyl chloride | HCID 2758535 | 94.4% |
반응 단계
78 g of thionyl chloride were added to 50 g of 3,4-dimethylbenzoic acid and the reaction mixture was heated at reflux for 3 hours. The reaction mixture was subsequently concentrated, and the residue was taken up twice in toluene and concentrated again. 53 g of 3,4-dimethylbenzoyl chloride were obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05547967 |
| 출처 데이터셋 | uspto-grants-1996_08 |
| ORD ID | ord-10b2432107f14a44882b92f914b359dc |
| 출처 메모 | uspto-grants-1996_08 |