1,3-Butadiene → 3-Methoxytoluene

HRID 1079088노트

반응식

HRID 1079088 반응식
C=CC=C.[CH3:5][O:6][C:7]1[CH:8]=[C:9]([CH2:13]CC=CC)[CH:10]=[CH:11][CH:12]=1>O>[CH3:5][O:6][C:7]1[CH:8]=[C:9]([CH3:13])[CH:10]=[CH:11][CH:12]=1

참가 물질

4

반응물 2

HCID 78451,3-ButadieneHCID 54500863HCID 54500863, 화합물

생성물 1

HCID 75303-Methoxytoluene수율 79%

시약·촉매·용매 1

HCID 962Water용매

반응 조건

온도
110 °C

실험 절차

After the flask was heated at a temperature of 110° C. during stirring in order to disperse the catalysts, 1,3-butadiene was fed for 6 hours at a flow rate of 0.3 mol/hour in order to promote the addition reaction. After the completion of the reaction, water was added to deactivate and separate the catalysts. The thus obtained reaction mixture was analyzed by gas chromatography. The results indicated that 5-(3-methoxyphenyl)-2-pentene was produced at 79% yield with respect to the consumed m-methoxytoluene.

후처리

  1. additionthe addition reaction
  2. additionwas added to deactivate and
  3. customseparate the catalysts
  4. customThe thus obtained reaction mixture

출처 및 근거

ORD 기록
ord-336e05441973463c9caf17c37b31a4a0
출처 데이터셋
uspto-grants-1996_08
특허 번호
US05550284

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