Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Ethyl-4'-iodobiphenyl → N,N'-di-p-tolyl-N,N'-di(4'-ethylbiphenyl-4-yl)-3,3'-dimethylbenzidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Ethyl-4'-iodobiphenyl | HCID 15477828 | — |
| 반응물 | N,N'-di-p-tolyl-3,3'-dimethylbenzidine | HCID 19428741 | — |
| 생성물 | N,N'-di-p-tolyl-N,N'-di(4'-ethylbiphenyl-4-yl)-3,3'-dimethylbenzidine | HCID 19428732 | 23.7% |
반응 단계
According to the same manner as that described in Synthesis Example 1, 14.9 g of N,N'-diacetyl-3,3'-dimethylbenzidine was reacted with 21.8 g of para-iodobenzene to give N,N'-di-p-tolyl-3,3'-dimethylbenzidine. Further, 12.0 g of N,N'-di-p-tolyl-3,3'-dimethylbenzidine was reacted with 15.4 g of 4-ethyl-4'-iodobiphenyl according to the same manner as that described in Synthesis Example 1 to give N,N'-di-p-tolyl-N,N'-di(4'-ethylbiphenyl-4-yl)-3,3'-dimethylbenzidine (hereinafter referred to as 6-c) (8.82 g, yield: 23.7%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05550290 |
| 출처 데이터셋 | uspto-grants-1996_08 |
| ORD ID | ord-8f99adbaebd0477fa6dbca77655fc277 |
| 출처 메모 | uspto-grants-1996_08 |