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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1079108생성일: 2026년 10월 26일

4-Ethyl-4'-iodobiphenyl → N,N'-di-p-tolyl-N,N'-di(4'-ethylbiphenyl-4-yl)-3,3'-dimethylbenzidine

https://huagongshe.com/reaction/1079108

반응식

참여 물질

역할이름HCID투입량
반응물4-Ethyl-4'-iodobiphenylHCID 15477828—
반응물N,N'-di-p-tolyl-3,3'-dimethylbenzidineHCID 19428741—
생성물N,N'-di-p-tolyl-N,N'-di(4'-ethylbiphenyl-4-yl)-3,3'-dimethylbenzidineHCID 1942873223.7%

반응 단계

According to the same manner as that described in Synthesis Example 1, 14.9 g of N,N'-diacetyl-3,3'-dimethylbenzidine was reacted with 21.8 g of para-iodobenzene to give N,N'-di-p-tolyl-3,3'-dimethylbenzidine. Further, 12.0 g of N,N'-di-p-tolyl-3,3'-dimethylbenzidine was reacted with 15.4 g of 4-ethyl-4'-iodobiphenyl according to the same manner as that described in Synthesis Example 1 to give N,N'-di-p-tolyl-N,N'-di(4'-ethylbiphenyl-4-yl)-3,3'-dimethylbenzidine (hereinafter referred to as 6-c) (8.82 g, yield: 23.7%).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05550290
출처 데이터셋uspto-grants-1996_08
ORD IDord-8f99adbaebd0477fa6dbca77655fc277
출처 메모uspto-grants-1996_08