Diisopropyl Ether → HCID 15839968, 화합물

HRID 1079456노트

반응식

[O:1]([CH:8]([CH2:12][CH3:13])[C:9]([OH:11])=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[N+]([O-])(O)=O.[O:18]([CH2:22][CH2:23][NH2:24])[N+:19]([O-:21])=[O:20].C(OC(C)C)(C)C>>[O:18]([CH2:22][CH2:23][NH:24][C:9](=[O:11])[CH:8]([O:1][C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1)[CH2:12][CH3:13])[N+:19]([O-:21])=[O:20]

참가 물질

반응물 3

HCID 7914Diisopropyl Ether

HCID 579872-Phenoxybutanoic acid

HCID 78397Ethanol, 2-amino-, 1-nitrate, nitrate (1:1)

생성물 1

HCID 15839968HCID 15839968, 화합물수율 57.8%

실험 절차

Following a similar treatment to that in Example 2 and using 0.64 g of 2-phenoxybutyric acid and 0.60 g of 2-nitroxyethylamine nitrate, 0.55 g of the title compound was obtained as colorless acicular prisms (solvent for recrystallization; diisopropyl ether).

출처 및 근거

ORD 기록: ord-e96571ea6213479b8cde6640c4779d1e
출처 데이터셋: uspto-grants-1996_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05580893

반응 노트

불러오는 중…