Diisopropyl Ether → HCID 15839974, 화합물

HRID 1079462노트

반응식

HRID 1079462 반응식
[CH3:1][C:2]1[O:6][N:5]=[C:4]([O:7][CH2:8][C:9]([OH:11])=O)[CH:3]=1.[N+]([O-])(O)=O.[O:16]([CH2:20][CH2:21][NH2:22])[N+:17]([O-:19])=[O:18].C(OC(C)C)(C)C>>[O:16]([CH2:20][CH2:21][NH:22][C:9](=[O:11])[CH2:8][O:7][C:4]1[CH:3]=[C:2]([CH3:1])[O:6][N:5]=1)[N+:17]([O-:19])=[O:18]

참가 물질

4

반응물 3

HCID 7914Diisopropyl EtherHCID 78397Ethanol, 2-amino-, 1-nitrate, nitrate (1:1)HCID 4962137Acetic acid, [(5-methyl-3-isoxazolyl)oxy]- (9CI)

생성물 1

HCID 15839974HCID 15839974, 화합물수율 36.9%

실험 절차

Following a similar treatment to that in Example 2 and using 0.40 g of 5-methyl-3-isoxazolyloxyacetic acid and 0.43 g of nitroxyethylamine nitrate, 0.23 g of the title compound was obtained as colorless needles (solvent for recrystallization; diisopropyl ether).

출처 및 근거

ORD 기록
ord-1dcef0ab2bc547b1944a332cf5a0dafe
출처 데이터셋
uspto-grants-1996_12
특허 번호
US05580893

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